粉末冶金铁基烧结炉的现状与展望

评述了国内外粉末冶金铁基烧结炉的发展动向和具体改进装备。即功能带设计、脱蜡装置,烧结带气氛控制,淬火带的设想,加热元件配置及新型可塑性耐火材料。     

微波热液法制备光催化TiO2功能材料

采用微波加热法，研究了钛配离子热分解水解反应的规律。结果表明，水解产物在大气气氛和300℃下煅烧2h，所得产物为锐钛型TiO2粉末。在紫外线照射下，乙酸经Ti02光催化反应12h后，残余量小于初始量的20％。     

湘潭新大粉末冶金设备制造有限公司的一体化真空烧结炉

简要介绍了湘潭新大粉末冶金设备制造有限公司研制的一体化真空烧结炉的炉子结构、脱蜡系统、工艺气体的引入系统、设备的控制系统以及炉子性能的鉴定结果。     

砂岩储集层微波加热产生微裂缝的机理及意义

微波加热无需介质传热,具有升温速度快、热惯性小、选择性加热、穿透力强、过程易于控制等优点,已被试验性地应用于石油开采中。但有关微波加热对储集层岩石微观结构影响的研究还很缺乏,限制了该项技术在油气开采领域的广泛应用。通过实验手段研究了微波加热前后砂岩岩样微观结构变化、微裂缝产生机理及特征。结果表明,砂岩在微波加热过程中容易产生微裂缝,且不同岩石的微波加热致裂机理不尽相同,主要包括:矿物失水收缩、颗粒粒间开裂和颗粒内部开裂,低渗透致密砂岩刚性颗粒的粒内开裂作用显著。微波加热产生的微裂缝具非定向特征,即使在应力的作用下有一部分裂缝会发生闭合,但仍有大量微裂缝可以起到增加渗透率的作用。井下微波加热的致裂作用有助于改善近井区域渗流能力,提高低渗透油气藏的开采效率。图4参15     

高合金铁基烧结材料在轧钢导位中的应用研究

本文研究了高合金铁基烧结材料在轧钢导位中的应用。实验表明,通过粉末冶金液相烧结技术,可以获得具有优良综合性能的制品,材料密度ρ≥7.5 g/cm3,硬度≥55 HRC,抗弯强度≥1 000 MPa,冲击韧度αk≥3.9 J/cm2,满足了轧钢导位辊的工作要求。材料利用率可达95%以上、降低了制备成本。使用寿命是普通轧辊寿命的3~6倍,适用于线材和小型型材的轧钢生产。     

浅谈烧结点火器与节能途径

本文论述了烧结点火器结构与烧结有关的节能途径     

Development of High Thermal Conductivity Aluminum Nitride Ceramic

AIN ceramics with densities varying from 3.18 to 3.30 g/cm³ and room-temperature thermal conductivities varying from 88 to 193 W/m K were produced. Different sintering conditions, packing powders, AIN powder sources, carbon additive, and sintering times were evaluated, and the key processing parameters which cause the differences in density and thermal conductivity were identified. SEM, TEM, and EDS were used to characterize the correlation between thermal conductivity, microstructure, and processing parameters. The important parameters which control the thermal conductivity of AIN ceramics are discussed.     

脉冲功率器件直流和动态热特性探测

介绍了针对影响微波脉冲功率器件可靠性的热性能问题，应用红外热分析技术。对比探测微波脉冲功率器件在动态和直流状态下的温度分布，峰值结温，热阻及其变化规律。     

Effects of Heat Treatment Temperature and Time on Structure and Static Magnetic Property of W-type Ferrite Hollow Mierospheres

Hollow spheres of hexagonal ferrite BaCozFelrO27 were fabricated through a spray pyrolysis technique using co-precipitation ferrite powder precursor as materials, followed by calcinations in an air atmosphere. The phase composition, micro-morphology, and static magnetic property of the particles were measured by XRD, SEM, and VSM. The results indicate that the method for preparation of ferrite hollow microspheres （FHM） results in a broad particles size distribution. The density of FHM decreased from 5.31 g/ cm^3 to 2.31 g/cm^3. When the heating rate was 5℃/min, and temperature was 1 200℃ for 4 hours, pure W-type ferrites were formed. With the heat treatment temperature and time increasing, the crystal structure becomes perfect, the saturation magnetization is increased and the coercive force is decreased.